The recrystallization technique was used to prepare submicron 3,3’-diamino-4,4’-azofurazan (DAAzF) with good performance, and DAAzF/VitonA polymer-bonded explosive (PBX) was prepared using solvent-slurry technique. The morphology and structure, as well as thermal property of samples were characterized and analyzed, and the apparent activation energy of thermal explosion was calculated．The results show that the particle size of DAAzF prepared at 0°C is smaller than that prepared at 35°C and 50°C. The apparent activation energy of the obtained PBX (650μm) is 182.68kJ·mol-1, indicating the better thermal stability than that of raw DAAzF.
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